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Copper vanadate nanoribbons were synthesized via a hydrothermal method and served as surface-enhanced Raman scattering substrates with an enhancement factor of 1450 in the detection 1 × 10-5 M Rhodamine 6 G solution. This substrate also exhibited satisfied results in the non-functionalized bio-detection of 1 × 10-2 M tyrosine solution, owing to its interaction to amino acids and vast surface area to further the interaction.