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Note: Circuit design for direct current and alternating current electrochemical etching of scanning probe microscopy tips

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3 Author(s)
Jobbins, Matthew M. ; Department of Chemistry and Biochemistry, University of Notre Dame, Notre Dame, Indiana 46556, USA ; Raigoza, Annette F. ; Alex Kandel, S.

Your organization might have access to this article on the publisher's site. To check, click on this link:http://dx.doi.org/+10.1063/1.3695001 

We present control circuits designed for electrochemically etching, reproducibly sharp STM probes. The design uses an Arduino UNO microcontroller to allow for both ac and dc operation, as well as a comparator driven shut-off that allows for etching to be stopped in 0.5–1 μs. The Arduino allows the instrument to be customized to suit a wide variety of potential applications without significant changes to hardware. Data is presented for coarse chemical etching of 80:20 platinum-iridium, tungsten, and nickel tips.

Published in:
Review of Scientific Instruments  (Volume:83 ,  Issue: 3 )

Date of Publication: Mar 2012

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