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Deposition of magnetite on AgI-silica core-shell particles by homogeneous precipitation method

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9 Author(s)
Kobayashi, Y. ; Dept. of Biomol. Functional Eng., Ibaraki Univ., Hitachi, Japan ; Fujisaku, T. ; Ayame, T. ; Nakagawa, F.
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A method for magnetite-deposition on Agl-SiO2 core- shell (Agl/SiO2) particles is proposed. A colloid solution of 1.0×10-3 M Agl nanoparticles was prepared mixing silver perchlorate at 1.0×10-3 M and potassium iodide at 2.0×10-3 M at 5°C, and then adding 3-mercaptopropyltrimethoxysilane at 4.5×10-5 M at 20°C. Agl/SiO2 particles with an average size of 42.7±10.3 nm and a Agl core size of 23.5±5.8 nm were prepared using a Stober method at 20°C in water/ethanol solution with 8.0×10-3 M tetraethylorthosilicate and 1.1×10-3 M NaOH in the presence of 1.0×10-3 M Agl nanoparticles. Preparation of magnetite nanoparticle colloid solution was performed with a homogeneous precipitation method using 5.0 M urea aqueous solution and 1.0×10-2 M iron chloride aqueous solution with Fe2+/Fe3+ molecular ratios of 1/0, 2/1, 1/2 and 0/1 in (50/50) (v/v) water/1-propanol solution at 80°C. Magnetite that revealed ferromagnetic property were produced using the ratios of 1/0, 2/1 and 1/2. Magnetite-deposition on the Agl/SiO2 particles was performed preparing the magnetite by the homogeneous precipitation method using 1.0×10-2 M iron chloride and 5.0 M urea in the presence of the Agl/SiO2 particles ([Agl] = 2.0×10-4 M). Tiny magnetite nanoparticles were deposited on the Agl/SiO2 particle surface. The magnetite-deposited Agl/SiO2 particles were ferromagnetic, and were drawn close to magnet. These results confirmed that the homogeneous precipitation method was suitable to magnetite-deposition.

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Nanoscience, Engineering and Technology (ICONSET), 2011 International Conference on

Date of Conference:

28-30 Nov. 2011

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