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Use of TiO2 modified-zeolite to obtain a multiwalled carbon nanotubes based composite electrode is presented in this study. The zeolite-modified TiO2 material was synthesized by solid-solid method and characterized by specific structural (XRD, DRUV-VIS) and morphological (SEM/EDX) methods. SEM image of composite electrode revealed a relative uniform distribution and orientation of the multiwalled carbon nanotubes and TiO2 modified-zeolite particles in epoxy matrix. The electroactive area of the composite electrode was determined using classical ferrocyanide method.