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Analysis of the Detection of Organophosphate Pesticides in Aqueous Solutions Using Hydrogen-Bond Acidic Coating on SH-SAW Devices

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4 Author(s)
Mensah-Brown, A.K. ; Dept. of EECE, Marquette Univ., Milwaukee, WI, USA ; Mlambo, D. ; Josse, F. ; Schneider, S.C.

The work presented in this paper focuses on the synthesis and characterization of a hybrid organic/inorganic chemically sensitive layer for rapid detection and analysis of OPs in aqueous solutions using SH-SAW devices. Coated SH-SAW devices on 36° YX-LiTaO and 42.75° YX-Quartz (ST-90° X Quartz), are used to determine the optimum operating conditions for achieving rapid sensor responses with high sensitivity. Three analytes (parathion-methyl, parathion, and paraoxon), having similar molecular mass and volume, are used to evaluate the performance of the hybrid organic/inorganic coating in terms of sensor properties of interest including sensitivity, selectivity, reproducibility. It is shown that the coating has a high degree of partial selectivity and sensitivity towards the analytes. With the present non-optimized chemical sensor, a limit of detection of 60 (ppb), 20 (ppb) and 100 (ppb) is estimated for parathion-methyl, parathion, and paraoxon, respectively, when using a 0.5 -thick BPA-HMTS sensing layer. Concentrations as low as 500 (ppb) parathion have been measured. This concentration is significantly much lower than the typical concentrations found on agricultural produce (≥10 ppm).

Published in:

Sensors Journal, IEEE  (Volume:12 ,  Issue: 5 )

Date of Publication:

May 2012

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