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Nanodithiocarbamate (DTC) complexes have been prepared by the reaction between DTC and metal salt under ultrasound irradiation. The DTC complex nanoparticles have been prepared in water. The antimicrobial activity of nanoparticles derivatives are tested against microorganism and compared with non-nano conditions. The resulting nanoparticles were characterised by X-ray diffraction and scanning electron microscopy.