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Single crystals of Sr1.5Ba0.5Zn2Fe12O22 were grown from the flux systems of BaCO3, SrCO3, and Na2CO3 by a high temperature, slow cooling, flux method. X-ray diffraction confirmed that the crystal structure is an extended single crystalline array of Zn-Y composition with an in-plane easy axis crystallographic orientation. The obtained single crystals were characterized for magnetic and microwave properties. The anisotropy field (HA) and the in-plane magnetization (σs) were 10 kOe and 22.5 emu/g, respectively. Ferrimagnetic resonance (FMR) measurements showed 41 Oe of linewidth (ΔH ) at 10 GHz.