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A simple external resistance heating diamond anvil cell and its application for synchrotron radiation x-ray diffraction

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6 Author(s)
Fan, Dawei ; Institute of Geochemistry of Earth’s Deep Interior Materials and Fluid Interaction, Chinese Academy of Sciences, Guiyang 550002, China ; Zhou, Wenge ; Shuyi Wei ; Liu, Yonggang
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A simple external heating assemblage allowing diamond anvil cell experiments at pressures up to 34 GPa and temperatures up to 653 K was constructed. This cell can be connected to the synchrotron radiation conveniently. The design and construction of this cell are fully described, as well as its applications for x-ray diffraction. Heating is carried out by using an external-heating system, which is made of NiCr resistance wire, and the temperature was measured by a NiCr–NiSi or PtRh–Pt thermocouple. We showed the performance of the new system by introducing the phase transition study of cinnabar (α-HgS) and thermal equation of state study of almandine at high pressure and temperature with this cell.

Published in:

Review of Scientific Instruments  (Volume:81 ,  Issue: 5 )

Date of Publication:

May 2010

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