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In-situ characterization of the amorphous to microcrystalline transition in hot wire CVD growth of Si:H using real time spectroscopic ellipsometry

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4 Author(s)
Levi, D.H. ; Nat. Renewable Energy Lab., Golden, CO, USA ; Nelson, B.P. ; Perkins, J.D. ; Moutinho, H.R.

We have used in-situ real-time spectroscopic ellipsometry (RTSE) to characterize the morphology and crystallinity of hot-wire CVD (HWCVD) Si:H films as a function of hydrogen dilution R=[H]/[H+SiH4], substrate temperature Ts, and film thickness db. Transitions from one mode of film growth to another are correlated with changes in the magnitude of the surface roughness during growth. The degree of crystallinity of the film can be determined from the form of the dielectric function. We have studied the growth parameter space for R from 0 to 14, Ts of 250°C and 500°C, and db from 0 to 1 μm. We have mapped out the crystallinity vs. R, Ts, and db based on our analysis of the RTSE data. These results have been corroborated using Raman scattering and atomic force microscopy to characterize the crystallinity and surface morphology of the films.

Published in:

Photovoltaic Specialists Conference, 2002. Conference Record of the Twenty-Ninth IEEE

Date of Conference:

19-24 May 2002

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